GCMS analysis results for sample AE03282, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.•Data File : C:\MSDCHEM\1\DATA\031902\3282.D Vial: 36 Acq On : 21 Mar 2002 11:07 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.11 1.16 ug/L 1252710 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91 3 7-CHLORO-1,3-DIHYDRO-5-PHENYL-2H... 342 C18H19C1N2OS1 000000-00-0 27 4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606S16 000540-97-6 23 Abundance Scan 1327 (15.112 mln): 3282.D (-) m/z 73.10 100.00% 73

5000 341

147 429 14.80 15.00 1520 1540 ‘T 45 117 I 179 207 251 281 3111 397 | - m/z 341.00 32.97% 01 Pr miz-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 ....................... ................ 5000 14*80 15.00 1520 15*40 m/z 147.10 13.89% 147 45 0- -1-+ 117 . 267' 300 207 . 250 . 200 ■ 311, 397, "i ■ ■ ■ • i • ■ miz-> 50 100 150 350 400 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73

14.80 15.00 15.20 15.40 5000 m/z 429.10 11.96% 341 429 147 45 117. [ 177 297 237 271 311 367 397 0- ‘ ' i ’ ■ II--p——pfrr m/z—> 50 100 150 200 250 300 350 400 Abundance#291536: 7-CHLORO-1,3-DIHYDRO-5-PHENYL-2H-1,4-DIBENZODIAZE: 73 341 ‘ I TT T T 14.80 15.00 15.20 15.40 m/z 342.00 11.48%

5000

45 .............. /.................... 0 • • i • • , +416.116,, 199. T>, 228299—,4PP—— m/z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40

3282.D 5080302.M Mon Mar 25 09:05:12 2002 Page 5

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