NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11
Acq On 4 Mar 2002 6:27 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
15.14 3.28 ug/L 1479910 Naphthalene-d8 13.05
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Cyclohexasiloxane, dodecamethyl-... 444 C12H36O6Si 000540-97-6 91
2 Cyclohexasiloxane, dodecamethyl- 444 C12H36 Si6 000540-97-6 72
3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DI 4812 000000-00-0 33
4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 16
Abundance Scan 1330 (15.140 min): 2339.D (-) m/z 73.10 100.00%
73
5000
341
147 429 14.80 15.00 15.20 15.40 ~
45
117
0- — ** i • r-f । rm *r
177 207 251 281 311
fr* P* rn 397 1 m/z 341.00 38.93%
m/z-> 50 100 150 200 250 300 350 400
Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc...
73
341
429 . ........... ..
5000'
14.80 15.66 15.20 15*40 '
m/z 147.10 15.06%
147
45 117 [ 297 267 311 397.
m/z->
0- .... 1 1 » '» «’ » J I I I "f I *1 I 1 I I rm
50 100 150 200 250
eh
300 350 400 '
Abundance #352522: Cyclohexasiloxane, dodecamethyl-
73
14.80 i5.'00 15.26 15.40 ''1
5000 m/z 429.10 13.56%
341
429
147
45 117 [ 177 207 237 271 311 367 397
0 * 'iI 11 ' * । •da • » । f । » . IT*r*rr, 367
1 1 r 397
i ■] r 1
m/z—> 50 100 150 200 250 300 350 400
Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHEN Y 1
73 180 H ‘ i ' ' ‘ ' l ‘ ■ I ‘ ‘ ' l
14.80 15.00 15.20 15.40
m/z 342.00 13.17%
5000
341
45
,106 149 I | 222 268 310,
0 1 n 1 '11 ' m-mputui f 1 1 ? , ■ rin rh/*nB/11
n/z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40 ‘
2339.D 5080302.M Mon Mar 18 08:32:40 2002 Page 5
NYC-WTC_000010619
OCR can misread numbers and units. Confirm readings against the page image before using them.