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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\030402\2339.D Vial: 11 • Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 3 - Isopropoxy- 1,1,1,7,7,7-he... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.87 2.30 ug/L 1125950 Acenaphthene-dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207S17 071579-69-6 59 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 53 3 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H3805Si6 000995-82-4 47 4 1,1,3,3,5,5,7,7,9,9,11,11-DODECA... 430 C12H38O5Si6 000000-00-0 47 Abundance Scan 1631 (17.870 min): 2339.D (-) m/z 73.10 100.00% 73

5000 147 281 . ' • i1 ■ ■ • I 111111121 327 17.60 17.80 18.00 18.20 01 — +117.193721, 117 .38315— ‘T m r fi । ri j n i . । । 1 . . m/z 147.10 37.03% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73

5000 1_____ - ‘ * I * ' • » I • ’ ■ ■ i ■ • • ■ i 147 17.60 17.80 18.00 18.20 m/z 281.10 34.10% 43 221 0+ IAdsyui T 327 415 TTmmmmg 519 sei m/z-> 50 100 150′200 2501 300 350 400 450 500 550 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

■ I " “ I " 281 17.60 17.80 18.00 18.20 5000 m/z 327.00 12.51%

369 207 90 m/z—> 0+ 7450— —10017150 200 250 BTT 177 1 249 mr 338 BBT 300 350 400 450 500 550 T T Abundance #347008: Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl 11111111 / A 111111111 73 17.60 17.80 18.00 18.20 m/z 282.00 9.87%

5000 281 207 133 103 [ 1771 , 251 341 A1E n/z—> 0 284450 me Tfmt 3111 ‘ I ’ ‘*1 rfi 111 । n 1111 > 111 । । > 1111 100 150 200 250 300 350 400 450 500 550 17.60 17.80 18.00 18.20 T

2339.D 5080302.M Mon Mar 18 08:32:42 2002‘ Page 6

NYC-WTC_000010620

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NYC-WTC_000010620Source: NYC Law Department, mirrored locally

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