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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010513–000010536

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data Pile C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 3-Isopropoxy-l,1,1,7,7,7-he... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.87 3.61 ug/L 1683240 Acenaphthene-dl0 18.17

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy- 1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 59 2 Pentasiloxane, dodecamethyl- 384 C12H36O4S15 000141-63-9 42 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 4 1,1,3,3,5,5,7,7,9,9,11,11-DODECA... 430 C12H38O5Si6 000000-00-0 32 Abundance Scan 1631 (17.870 min): 2334.D (-) m/z 73.05 100.00% 73

5000 147 281 1 1 । 1 1 1 1 14*i | । । r T’T 327 17.60 17.80 18.00 18.20 0+ - " I r’ 117 , 191221251 Tmpr ........................................................ m/z 147.10 36.44% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73

5000 1 • i ■ • ■11 rv* 1" '^i' " 147 17.60 17.80 18.00 18.20 m/z 281.00 33.99% 43 221 281 327 415 561 04 TTTTT T - 11111 f519 > + rr । t r m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #322221: Pentasiloxane, dodecamethyl- 73 147 281

17.60 17.80 18.00 18.20 5000 m/z 327.00 12.09% 369

207

m/z-> 0+ 334—444+*4+ 50 117 zL24 100 150 200 250 300 350 400 450 500 550 1111‘11111'111'' ' I'f Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 1111111| i A 111111111 73 147 17.60 17.80 18.00 18.20 m/z 282.10 9.51% 281 5000

369 207 9A0 m/z—> 0 7’4 50 117 Tirifr 177,120 338 i r. ।....,» r r 11 >»»»1111111 > 111 > । 100 150 200 250 300 350 400 450 500 550 1'1 I “ '11 ’ —IBWTITT 17.60 17.80 18.00 18.20

2334.D 5080302.M Mon Mar 18 08:30:57 2002 Page 7

NYC-WTC_000010524

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NYC-WTC_000010524Source: NYC Law Department, mirrored locally

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