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GCMS analysis report, sample AE02336, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010558–000010576

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

•_ Data File C:\MSDCHEM\l\DATA\030402\2336.D Vial: 8 Acq On 4 Mar 2002 4:00 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 3-Isopropoxy-l, 1,1,7,7,7-he... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.87 1.41 ug/L 693586 Acenaphthene - dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Isopropoxy-1,1,1,7,7,7-hexamet. . . 576 C18H5207Si7 071579-69-6 64 2 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 36 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 35 4 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H38O5Si6 000995-82-4 32 Abundance Scan 1631 (17.870 mln): 2336.D (-) m/z 73.10 100.00% 73

5000 147 281 TITPITTT ITT 327 17.60 17.80 18.00 18.20 TTTrfem 4 191221251 m/z-> ol - —117 50 100 150 200 250 300 350 400 450 500 550 m/z 147.10 36.74%

Abundance #379639:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73

5000 ■11 • • ■ ■ i ’ 1*’ ■ ■ i ■ ■ 147 17,60 17.80 18.00 18.20 m/z281.00 36.12% 43 221 281 327 415 519 561 miz-> 04 — • 11 • । ■ i ■ ■ • • । f ■ 11 ■ • 11 Ah 1' “ 111 > ■ I < । ■ ■ l'il ■ ■ l ■ 50 100 150 200 250 300 350 400 450 500 550 Abundance #322221: Pentasiloxane, dodecamethyl- 73 147 281

17.60 17.80 18.00 18.20 5000 m/z 327.00 12.27% 369

207 117 33 । * । T 04 imfrt — .... 177,1249 f, p f p nf. r. ।.. 111* ’ 11/11/611/2/0/1/"B//1/B.T m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147 T T T T 17.60 17.80 18.00 18.20 m/z 282.10 10.06% 281 5000

369 207 ,,Q

/z—> 0 27 ] ( tmimen 50 117 17L241, 338 J............................... 100 150 200 250 300 '350' 400 450 500 550 11111 ■ ■ I • Tj ». r. । . y 17.60 17.80 18.00 18.20

2336.D 5080302.M Mon Mar 18 08:31:45 2002 Page 5

NYC-WTC_000010567

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NYC-WTC_000010567Source: NYC Law Department, mirrored locally

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