GCMS analysis report for sample AE02335, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Benzoic acid, 4-ethoxy-, et... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

18.79 0.46 ug/L 212739 Acenaphthene-dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H1403 023676-09-7 95 2 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H14O3 023676-09-7 95 3 1,3-Cyclohexadiene-l-carboxylic ... 194 C12H1802 035044-59-8 59 4 Benzoic acid, 4-hydroxy-, ethyl ... 166 C9H10O3 000120-47-8 49 Abundance Scan 1733 (18.795 min): 2334.D (-) m/z 121.10 100.00% 121

149 5000 65 138 194 93 —PPTTTTT 166 18.40 18.60 18.80 19.00 19.20 —4 _ | 199. 1........ I. 76 50 J h m/z 149.10 52.07% Of ’IS**’I* . hi, I Il— m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #105823: Benzoic add, 4-ethoxy-, ethyl ester $$ Benzoic a.,. 121

149 5000 18.40 18.60 18.80 19.00 19.20 138 194 m/z 194.10 31.43% 29 65 93 166 0! 15,1 * I 50 J 76 | 109 I ’,I ., XI » ,. J, 1» . ’ 179I* ’ I l . 'I • • ' * i-*— m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #105824: Benzoic acid, 4-ethoxy-, ethyl ester 121 _- 149 18.40 18.60 18.80 19.00 19.20 m/z 138.10 28.37% 5000 194 65 138 93 166 J 109 Of 11101 -r+fT-r 76 179 miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #106441: 1,3-Cyclohexadiene-1 -carboxylic add, 2,6,6-trime... 107 121 T 1 167111 18.40 18.60 18.80 19.00 19.20 m/z 65.10 27.31%

5000 29 91 149 194 41 77 135 65 Tr pL 4—l . 4 r he 53 ’11, II 1406 165 179 , 0 • ■ i ‘ ' । । i • ‘ * * i T m/z—> 20 40 60 80 100 120 140 160 180 200 18.40 18.60 18.80 19.00 19.20

2334.D 5080302.M Mon Mar 18 08:30:58 2002 Page 8

NYC-WTC_000010525