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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037859
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Benzoic acid, 4-ethoxy-, et... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 18.77 1.37 ug/L 786733 Acenaphthene-d10 18.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H1403 023676-09-7 97 2 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H1403 023676-09-7 96 3 Benzoic acid, 4-hydroxy-, ethyl ... 166 C9H1003 000120-47-8 64 4 Ethvinaraben 166 C9H1003 000120-47-8 58 undance Scan 1730 (18.768 min): 220LB.D (-) m/z 121.10 100.00 11

5000 149 65 138 194 93 166 18.40 18.60 18.80 19.00 76 109 179 m/z 149.10 46.59 -> 20 40 60 80 100 120 140 160 180 200 bundance #105823: Benzoic acid, 4-ethoxy-, ethyl ester $$ Benzoic a... 11

149 5000 18.40 18.60 18.80 19.00 138 194 m/z 65.10 30.33 29 65 93 166 0 15 1 1l., 76 109 179 -> 20 40 60 80 100 120 140 160 180 200 undance #105824: Benzoic acid, 4-ethoxy-, ethyl ester 11

149 18.40 18.60 1 .80 19.00 5000 m/z 194.10 30.24 194 65 138 93 166 76 109 179 0 -> 20 40 60 80 100 120 140 160 180 200 bundance #67030: Benzoic acid, 4-hydroxy-, ethyl ester (CAS) $$ Eth... 11 18.40 18.60 18.80 19.00 m/z 138.10 27.22

5000

39 65 93 138 166 53 0 nlz-> 20 40 60 80 100 120 140 160 180 200 18.40 18.60 18.80 19.00

7')nT.R n mnun9n9 M Th., Mir 99 9 9 . ) .94 ')nn) Dane R

NYC-WTC 000037859

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NYC-WTC_000037859Source: NYC Law Department, mirrored locally

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