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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037858
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

0 Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 17.84 4.00 ug/L 2293480 Acenaphthene-d10 18.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 53 2 (trimethylsilyloxy) 2-(trimethy... 398 C18H27ClO4Si2 000000-00-0 28 3 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 28 4 Hexasiloxane, 1,1,3,3,5,5,7,7,9.... 430 Cl2H38O5Si6 000995-82-4 17 undance Scan 1628(17.842 min): 220LB.D (-) m/z 73.10 100.00%

5000 147 281

327 17.60 17.80 18.00 1820 117 1911251 383415 m/z 147.10 37.20 0 -> 50 100 150 200 250 300 350 400 450 500 550 undance #322218: Trisiloxane,1,1,1,5,5,5-hexamethyt-3,3-bis[(trim... 3 17

281 5000 17.60 17.80 18.00 18.20 m/z 281.00 33.80 369 27 117 1777 249 338 0 -> 50 100 150 200 250 300 350 400 450 500 550 undance #330901: (trimethylsilyloxy) 2-(trimethyisityloxy)-6-oxo-...

1 1 1 , 1 , I I I

17.60 17.80 18.00 18.20 5000 m/z 327.00 12.24 147 281 191 I 398

ntz-> undance 0 50 100 150 200 250 300 350 400 450 500 550 #379639: 3-tsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-Ms(tr... 1k 17.60 17.80 18.00 18.20 m/z 282.10 9.90

5000 147 43 221 281 327 415 519 561 0 50 100 150 200 250 300 350 40Q 450 500 550 17.60 17.80 18.00 18.20

')')AT T CARA'ZA') M 11„• M . 'l 11 .r' .77 ')AA7 De,,n 7

NYC-WTC 000037858

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NYC-WTC_000037858Source: NYC Law Department, mirrored locally

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