GCMS analysis results for sample AE03805, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\031902\3805.D Vial: 15 Acq On : 19 Mar 2002 11:07 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 17.85 1.32 ug/L 637961 Acenaphthene-dl0 18.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 40 2 3-Isopropoxy-l,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 27 3 9,12,15-Octadecatrienoic acid, 2... 496 C27H5204Si2 055521-22-7 22 4 1,4-Bis((trimethylsilyl)acetynyl... 296 C18H24Si2 00000-00-0 20 Abundance Scan 1629 (17.851 min): 3805.D (-) m/z 73.10 100.00% 73

5000 281 147

327 TII—u —PP 17.60 17.80 18.00 18.20 117 191221251 —........ ... ....................... m/z 281.10 44.22% 0- wmmf miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

281 5000 T T T 17.60 17.80 18.00 18.20 m/z 147.10 40.00% 369 207 240

m/z-> 0- 24+ +H* 117 177 1 249 rme 50 100 150 200 250 300 350 400 450 500 550 ■ 338 [__________________ ‘ i ■r ■ • i ■ • ■ ■ i ■ ■ • ■ i ■ ■ • • i • ■

Abundance #379639: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 I ’ ‘ ‘ I * ‘ k ‘ I T 17.60 17.80 18.00 18.20 5000 m/z 327.00 17.59% 147 43 221 281 I I O&s 415 519 561 0- •' i ■ THmr - —— m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #367776: 9,12,15-Octadecatrienoicacid, 2,3-bis[(trimethyl... - 29 73 17.60 17.80 18.00 18.20 147 m/z 282.10 13.68% 220 5000 109

mtz-> OM 50 100 T 1 260uuairca2Z”s09,951463 150 200 250 300 350 400 450 500 550 17.60 17.80 18.00 18.20

OAr A6 m..

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