GCMS analysis results for sample AE03282, March 2002

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Library Search Compound Report

••Data File : C:\MSDCHEM\1\DATA\031902\3282.D Vial: 36 Acq On : 21 Mar 2002 11:07 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

17.85 1.11 ug/L 1291770 Acenaphthene-diO 18.15

Hit# of 5 Tentative ID. MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 50 2 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 38 3 (trimethylsilyloxy) 2-(trimethy... 398 C18H27C1O4S12 000000-00-0 23 4 9,12,15-Octadecatrienoic acid, 2... 496 C27H5204Si2 055521-22-7 22 Abundance Scan 1629 (17.851 min): 3282.D (-) m/z 73.10 100.00% 73

5000 281 147

327 ’'111 ■ T 1 /1 M 11 1 111 221 17.60 17.80 18.00 18.20

n/z-> 45 0- . I I 50 100 . 117 । . ’i 150 200 . r T*r —..., i 249 191 ।l, 250 I 18T e, - ■ 300 350 400 383415 m/z 281.10 44.56%

Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis((trim... 73 147

281 5000 17.60 17.80 18.00 18.20 m/z 147.10 40.67% 369 45 — 207 20 0- 95117 rr 1 P 177 [ 249। -Pr-ter 310 341 1 I 1 1 1 1 I ' ‘ 400 m/z-> 50 100 150 200 250 300 350 Abundance #322221: Pentasiloxane, dodecamethyl- 73 147 281

T Mjng 17.60 17.80 18.00 18.20 5000 m/z 327.00 17.12% 369

207

0- 45 -4+ L 117 ■■ 1 yit ■ r 1—- 177, 1249 300'350 400 m/z-> 50 100 150 200 250 Abundance #330901: (trimethylsilyloxy) 2-(trimethylsilyloxy)-6oxo-... * 73 1' 111 ■' i 17.60 17.80 18.00 18.20 m/z 282.10 11.48%

5000 147 281

0 ... Il 102 . 1 1 1 1 11 । । • > 191 1 • ■ ■ ' i • • • • i • ■ i 308 i__________ • i • ■ ■ • i • • 398 - Tl/Z-> 50 100 150 200 250 300 350 400 17.60 17.80 18.66 18*20

3282.D 5080302.M Mon Mar 25 09:05:14 2002 Page 6

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