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GCMS analysis results for sample AE03281, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.

NYC-WTC_000011415–000011428

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031902\3281.D Vial: 35 Acq On : 21 Mar 2002 9:11 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

17.85 0.77 ug/L 1058330 Acenaphthene-dl0 18.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4S15 003555-47-3 43 2 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 40 3 (trimethylsilyloxy) 2-(trimethy... 398 C18H27C104Si2 000000-00-0 38 4 Silane, [bicyclo[4.2.0]octa-3,7-... 282 C14H26O2Si2 036461-33-3 38 Abundance Scan 1629 (17.851 min): 3281.D (-) m/z 73.10 100.00% 73

5000 147 281

327 ■ ■ i ■ ■ ■ ■ i ibe* 4 > >. 221 17.60 17.80 18.00 18.20 04 — 117 Pr .1911214 383415 । 111 r । it ji । 1 » I m/z 147.10 42.15% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

281 5000 .. s 17.60 17.80 18.00 18.20 m/z 281.00 41.21% 369 207 940 44+ h-rtm Pi 177.24, 117 338 1 04 rn/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 • ■ 1 ■ • • i • • 17.60 17.80 18.00 18.20 5000 m/z 327.00 15.76% 147 43 221 281 327 415 miz-> O' 1' *1 11 *1 1 TI mm 50 100 150 200 250 300 350 400 450 500 550 519 561 1 > । ]■ । i 11 t r ।

Abundance #330901: (trimethylsilyloxy) 2-(trimethylsilyloxy>-6-oxo-... 73 17.60 17.80 18.00 18.20 m/z 282.10 12.14%

5000 147 281 191 I 398 0- I 1 i i_______ -rp-r-n-p-r _ ........ .................. • ‘ I ‘ ‘ ■ I ‘ ‘ '11" " I" ■' I ‘1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 17*60 17.80 18.00 18.20

3281.D 5080302.M Mon Mar 25 09:04:03 2002 Page 6

NYC-WTC_000011425

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NYC-WTC_000011425Source: NYC Law Department, mirrored locally

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