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GCMS analysis results for sample AE03281, March 2002

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Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.

NYC-WTC_000011415–000011428

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011424
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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\l\DATA\031902\3281.D Vial: 35 Acq On : 21 Mar 2002 9:11 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.11 1.12 ug/L 1440910 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606S16 000540-97-6 91 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4S12 000000-00-0 38 4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 37 Abundance Scan 1327 (15.112 min): 3281 .D (-) m/z 73.10 100.00% 73

5000 341 147 429 14.80 15.00 15.20 15.40 45 - 117, l) 177,207 251 281 311 4 0- 397— m/z 341.00 32.34% m/z-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000 . ............. 14.80 15.00 15.20 15.40 m/z 147.10 14.65% 147

0- 45 II. 117 207 .267—T 311 397. rn/z-> 50 100 150 200 250 300 350 400 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73 — T T 14.80 15.00 15.20 15.40 5000 m/z 429.10 11.08% 341 429 147 45 117 [ 177 207 237 271 311. 367 397 0 - TTIPPmmmmTTT+‘I4‘‘‘1** m/z—> 50 100 150 200 250 300 350 400 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY}-5-DEUTEROPHENf mTmTTT 73 180 14.80 15.00 15.20 15.40 m/z 342.00 10.79%

5000 341 45

0 , 106 149 P— | 222 268 ,310, , ... rn/z-> 50 200 ' 250 300 350 400 100 150 14.80 15.00 15.20 15.40

3281.D 5080302.M Mon Mar 25 09:04:01 2002 Page 5

NYC-WTC_000011424

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NYC-WTC_000011424Source: NYC Law Department, mirrored locally

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