NYC-WTC_000011415
Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS re-injection results, Sample 1639, Mar 2002
Machine-extracted title · confidence 100%Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
NYC-WTC_000012129–000012144Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
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NYC 9/11 Public Portal Document
Library Search Compound Report .•Data File : C:\MSDCHEM\1\DATA\031902\1640.D Vial: 25 Acq On : 20 Mar 2002 10:32 am Operator: McLean Sample ; RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cyclohexasiloxane, dodecame... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.11 1.95 ug/L 723724 Naphthalene-d8 13.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl-... 444 C12H36O6Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 72 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4Si2 000000-00-0 38 4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 32 Abundance Scan 1327 (15,112 min): 1640.D (-) m/z 73.10 /100.00% 73
5000 341 ■ ' i ■ ■ ■ I 1 ■ 11 ■ '1 ■ i 147 429 14.80 15.00 15.20 15.40
m/z-> 0- 50 -4+ 45 ' ■ i * 1 100 150 117 200 I 177.297 251 —It— 295 250 1 1' | r • • r । i । ■ . । . > 300 350 400 m/z 341.00 34.88%
Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethyc... 73 341
5000 429 .m 14.80 15.00 15.20 15.40 m/z 147.10 14.81% 147 45 . 207 . . 267 P 117 311 397. m/z-> Abundance — 0- g 100 150 200 350 400 250 #352522: Cyclohexasiloxane, dodecamethyl- 300 i • ■ • > T1 ' ”
73
’t4 T T T x 14.80 15.00 15.20 15.40 m/z 342.00 12.97% 5000 341 429 147 45 207 237 271 3111 0 TT . 117 1 17711--PTer 367 397 m/z-> 50 100 150i200 250 300 350 400 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHENf ..................... .................. 73 180 14.80 15.00 15.20 15.40 m/z 429.10 12.67% 1 5000 341 45 , 106 149 | 222 268 31°, A ...................................... 0- _ ii * ' I ‘ ■ Tt T*—nTOBTIr m/z-> 50 100 150 200 250 300 350 400 14*80 15.00 15.20 15.40 ‘
1640.D 5080302.M Thu Mar 21 06:31:26 2002 Page 4
NYC-WTC_000012137
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NYC-WTC_000012137Source: NYC Law Department, mirrored locally
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