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GCMS analysis results, Sample AE01647, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report for GC/MS analysis of sample AE01647 conducted on March 25, 2002.

NYC-WTC_000012182–000012193

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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Scanned page image, NYC-WTC_000012190
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\031902\1647.D Vial: 27 Acq On : 20 Mar 2002 12:10 pm . Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.11 0.91 ug/L 382971 Naphthalene-d8 13.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 52 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4Si2 000000-00-0 40 4 5-(2,3-BIS(TRIMETHYLSILYLOXY)PRO... 444 C20H40N205Si2 012774-38-8 33 Abundance Scan 1327 (15.112 mln): 1647.D (-) m/z 73.10 100.00% 73

5000 341 ...... । । / ...... । 75 I I | I | | | [ 147 429 14.80 15.00 15.20 15.40

m/z-> 0- —50L ’100/11717,207, 150 200 251 TPPtr 250 31 300 350 400 m/z 341.00 41.08%

Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000 T T .T T T 14.80 15.00 15.20 15.40 m/z 147.10 14.88% 147 45 117 207 r 267 311. 0- 1 1 11 I 1 11* 1 r1 '■ ' 1 H 1 ■ "i ■ ■ ■ 397. ■ i • • 50 100 150 200 250 300 350 400 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73 1 ' I ' ‘ " I'' • ■ i • • ■ ■ i ■ ■ ■ ■ । 14.80 15.00 15.20 15.40 5000 m/z 429.10 14.42% 341 429 147 45 117 1 177 207 237 271 3111 0 - TTImmmprr 367 397 m/z—> 50 100 150 200 250 300 350 400 ........... ............................ Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHEN / 73 180 14.80 15.00 15.20 15.40 m/z 342.00 13.66%

5000 341 45

0 1 *1" 1 , 106, ,14%, 1 222 268 310 1, . T T T /z—> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40

L647.D 5080302.M Thu Mar 21 06:32:06 2002 Page 4

NYC-WTC_000012190

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NYC-WTC_000012190Source: NYC Law Department, mirrored locally

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