GCMS reference analysis results for sample AE03265, March 2002

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Library Search Compound Report

. ‘Data File : C:\MSDCHEM\1\DATA\031902\3265FB.D Vial: 34 Acq On : 21 Mar 2002 8:13 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS ’Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyclohexasiloxane, dodecame... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.11 0.57 ug/L 591372 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 72 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4S12 000000-00-0 43 4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 37 Abundance Scan 1327 (15.112 min): 3265FB.D (-) m/z 73.10 100.00% 73

5000 341 147 429 14.80 15.00 15.20 15.40 45 — 117 [ 177 207 251 0- . 311 ! "I । .A r.ht ■ '• "i atut 1 ' I ' 1 1 ri 1 1 1 TT"8 •’“1 397L m/z 341.00 33.28% m/z-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000 ■ ■ i ■ • • i ■ ‘ ' i 14.80 15.00 15.20 15.40 m/z 147.10 14.75% 147 45 117 207 — 267 311 , n/z-> 0- 050 , —I 100 150 200 250 300 350 397. 400 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73 .............. . 14.80 15.00 15.20 15.40 5000 m/z 342.00 10.64% 341 429 147 45 117 397177 237 271 311 0' — TT——————m—TTTTT I 367 • ■ 1 * i •1 m/z—> 50 100 150 200 250 300 400350 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHEN / 73 180 mmm 14.80 15.00 15.20 15.40 m/z 429.10 10.42%

5000 341 45 310 m/z-> 0 —T ,106 .149 50 100 150 | 222 —Idem - 200 268 250 300 350 400 11I■> ■111 <■ mmPP 14.80 15.00 15.20 15.40

3265FB.D 5080302.M Mon Mar 25 09:02:39 2002 Page 4

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