GCMS analysis results for sample AE03805, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3805.D Vial: 15 Acq On : 19 Mar 2002 11:07 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.11 1.83 ug/L 806015 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91 3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4Si2 000000-00-0 38 4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 32 Abundance Scan 1327 (15.112 min): 3805.D (-) m/z 73.10 100.00% 73

5000 341 — . — 147 429 14.80 15.00 15.20 15.40 45 - 117 —f179 207 251 TIengrr nfrr 295 1 m/z 341.00 37.75% 0- TUr m/z-> 50 100 150 200 250 300 350 400 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341

429 5000' . 11’ ITri'rfTI " I " “ I 14.80 15.00 15.20 15.40 m/z 147.10 16.30% 147 45 117 207 267 3111 397, m/z-> 0- Abundance g TIIIT 100 150 200 250 300 350 #352522: Cyclohexasiloxane, dodecamethyl- 400

73 — • • i • ■ •' i ■ 14.80 15.00 15.20 15.40 m/z 429.10 13.30% 5000 341 429 147 45 ”, —I 117 , 177 207 237 271 311 r, i 367 397 0 ' —- — ■ ‘ ■ i r ' miz—> 50 100 150 200 250 300 350 400 Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHEN Y 73 180 T 11f i1' ■ ■ I 14.80 15.00 15.20 15.40 m/z 342.00 12.29%

5000 341 45

0 — 1106 ,149 1 222 268 31°t — • I 1 • • • 1 . . | T • ■ m/z-> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40

3805.D 5080302.M Thu Mar 21 11:49:05 2002 Page 5 NYC-WTC_000037973