GCMS analysis results for sample AE03805, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\3805.D Vial: 15 Acq On : 19 Mar 2002 11:07 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.05 1.12 ug/L 493651 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 76 3 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI... 573 C24H51NO5S15 000000-00-0 47 4 2-TRIMETHYLSILYLAMINO-l-TRIMETHY... 457 C20H43NO3Si4 068595-65-3 47 Abundance Scan 989 (12.046 min): 3805.D (-) m/z 73.10 100.00% 73

5000 267 355 .............. .................. 11.80 12.66 12.20 12.40 162193223 0- TT I ■125‘ T oL - 7 ---J . 323 m/z 267.00 35.37% i-.i IIt 11 I ' ‘* I miz—> 50 100 150 200 250 300, 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 i * * *' r e 11.80 12.00 12.20 12.40 T

m/z 355.10 23.35%

0- 207 4 , > । 323 > i*i I |h i i i । i । i i । i miz-> 50 100 150 200 250 ' 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

i' ' '1 I I • ■ • i T 11.80 12.00 12.20 12.40 m/z 356.10 8.77% 5000 267 355

281 . 103133163193223 1 0-.— TTTTTTTTr 3231................... m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance#379385: 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRIMETHYLSlLYLAMlNO- \ 73 i ‘ *1 ‘ f ■ ■ • i 11.80 12.00 12.20 12.40 m/z 268.00 8.53%

5000 355

0- 48.1123 117179 218251.221325, 396 440470 530560 • ‘ i ‘ • i ■ ■ • • i ' ■1 ■ i' ■ .... L T T m/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

?205 n EnR200 M Th1 Mar 21 11.40.04 2002 Pace 4 NYC-WTC_000037972