GCMS analysis results for sample AE02151, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031802\2151.D Vial: 29 Acq On : 20 Mar 2002 1:04 am Operator: McLean Sample : GC/MS SCAN 3/8 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.60 ug/L 234851 Naphthalene-d8 13.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 90 3 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI... 573 C24H51NO5S15 000000-00-0 47 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 989 (12.047 min): 2151. (-) m/ z 73.10 100 00% 73

5000 267 355 11.80 12.00 12.20 12.40 154 193273 323 m/z 267.00 32.08% 0- — TTI —1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ ■ l ■ 11.80 12.00 12.20 12.40 m/z 355.00 22.77%

L | 207 323, 0 — ■ ■i■■■■ i■■- ■i ■ ■■ ‘ i■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 —........ — 11.80 12.00 12.20 12.40 5000 m/z 74.10 8.39% 267

355

28 , 103133163193223 323 0 ' T '"i ' t 1 1 1 1 ' 1 i ' ' 1 ' i ' 1 1 ' i 1 1 ■ ' i ' 1 ■ ■ i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance#379385: 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRlMETHYLSILYLAMINO- - > ■ । ■ ■ ■ ■ । ■ 73 11.80 12.00 12.20 12.40 m/z 268.00 7.82%

5000 355

0 193147179 218 251 291 325 TTTT—u-/TTTuuLum 396 440470 530560 ' ' i ' ' ' ' i ' ■ < । 1 ■ ■ ■ । ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

2151.D 5080302.M Wed Mar 20 02:42:38 2002 Page 3

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