GCMS analysis results for sample AE03732, March 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031202\3732.D Vial: 58 • Acq On : 13 Mar 2002 3:35 am Operator: McLean Sample : SAMPLE 3732 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library s C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 036 ug/L 389554 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02- 2 Cyclopentasiloxane, /decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzoic acid, 2-[ (trimethylsilyl. . . 282 C13H2203Si2 003789-85-3 43 4 Phenethylamine, N^nethyl-.beta.,... 399 C18H37NO3S13 010538-35-9 37 Abundance Scan 990 (12.055 min): 3732.D (-) m/z 73.10 100.00% 73

5000 267 355 —... ......... 11.80 12.00 12.20 12.40 45 108 133154 193 223 . - 323 m/z 267.00 45.73% 0- T t — 1*+ —T*r ——1 11 m/z-> 50 100 150 200 250 300 350 Abundance - opentasiloxane, de am 70

5000 267 i • ■ ■ ■ i I" • ‘Jm 11.8012.0012.2012.40 355 m/z 355.10 37.98% 45 .1. i 0- ■26‘ ‘ 96 TTT 133 165 123 223 2474 293 323 , 4 m/z-> 50 100 150 ' 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

267 355 _ 11.80 12.00 12.20 12.40 5000 m/z 356.10 13.44%

45 207 , | 323 0- — • i • * - -------- I » Ir + i miz—> 50 100 150 200 250 300 350 Abundance #227684: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... _____ , \ .... ।, 73 >. । .... ।। 11.80 12.00 12.20 12.40 m/z 357.10 9.98%

5000 267

45

0 135 alTr 92115.11159, 123 233 i ■ •' ■ i i ■ ■ ■ ■ i m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

3732.D 5080302.M Fri Mar 15 14:27:07 2002 Page 3

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