GCMS analysis results, sample AE03730, March 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\031202\3730.D Vial: 56 Acq On : 13 Mar 2002 1:57 am Operator: McLean Sample : SAMPLE 3730 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 1.08 ug/L 452167 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 3 Benzoic acid, 2-[ (trimethylsilyl... 282 C13H2203Si2 003789-85-3 37 4 Benzoic acid/^-[ (trimethylsilyl... 282 C13H22O3Si2 003789-85-3 37 Abundance 7 Scan 990 (12.055 min): 3730.D (-) m/z 73.10 100.00% 73

5000 267 355 y 45 ‘' 11.66 12.00 12.20 12.40 m/z-> 01 - 50 ■ 100 i 133150154—23.223 ■ ■ 200 —250 300 323 1 + i ■ 350 m/z 267.00 43.23%

Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 11.80 12.00 12.20 12.40 355 m/z 355.10 37.89% 45 0- 26—1 96 TT 133 165.123 ,223 2474 293 323 , 1'L m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 TT । *'' • । ' i 355 11.80 12.00 12.20 12.40 267 m/z 356.10 13.88% 5000

45 323 207 it 0 — ‘ 1 I 1 T f i "• • T Tr + 1 miz—> Abundance 50 100 150 200 250 300 #227687: Benzoic add, 2-[(trimethylsilyl)oxy]-, trimethyl... 73 267 350 . L.. 111.80 12.66 12.20 12*40 m/z 268.00 10.06%

5000

135 193 0 _ 47., Tt I w 92 115.1444144233 1IT 300 ’ • • i • • • • i • ‘ 1’211115 m/z—> 50 100 150 200 250 350 11.80 12.00 12.20 12.40

3730.D 5080302.M Fri Mar 15 14:26:52 2002 Page 3

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