GCMS analysis results for sample AE03281, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031902\3281.D Vial: 35 Acq On : 21 Mar 2002 9:11 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.56 ug/L 724294 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 38 4 Benzeneacetic acid, .alpha.,4-bi... 384 C17H32O4S13 037148-64-4 38 Abundance Scan 990 (12.055 mln): 3281 .D (-) m/z 73.10 100.00% 73

5000 267 355 ‘//t//8norto1t1‘883 11.80 12.00 12.20 12.40 45 103 133 162 237, , m/z 267.00 46.12% 1 323 0- — 51* , "rd Pit .■ ■ " “i ah.;" rn/z—> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 j rp ■ > r । . . 11.80 12.00 12.20 12.40 355 m/z 355.10 36.46% 45 0- 26 , 1 ' 1 i 96 133 165,193 7223 247.1 293 323,1 miz-> 50 100 150' 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 T T • i ■ ‘ 355 11.80 12.00 12.20 12.40 267 m/z 356.10 13.23% 5000

m/z-> 0- ‘ 45 • I

50 I I ' 100 ' I

150 ‘ ‘ I 200 * ' ’ 250 ’ I ’ 300 • 207 350 vi r* ■■■ 2344 Abundance #227689: Benzoic add, 2-[(trimethylsilyl)oxy]-, trimethyl... 73 T T A— T 11.80 12.00 12.20 12.40 m/z 268.00 10.90%

267 5000

45 18 | 0- — "i 5* ,92,411444123233. ,4 * 1 • * m/z—> 50 100 150 200 250 300 350 1180 12.00 12.20 12.40 3281.D 5080302.M Mon Mar 25 09:03:59 2002 Page 4

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