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GCMS blank analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011355
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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.68 ug/L 748627 Naphthalene-d8 13.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 38 4 Benzoic acid, 2,5-bis(trimethyls. .. 370 C16H3004Si3 003618-20-0 35 Abundance Scan 990 (12.056 mln): 0214LB.D (-) m/ z 73.10 100.00% 73

5000 267 355 ********)* ** 45 11.80 12.00 12.20 12.40

/z-> 103 133154 .193223 1 [ 0- - *31//*/8-0trm3*Tt 50 100 150 200 250 300 323+1, 350 m/z 267 00 42.94%

Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 ■ ‘ ■ ■ I'''11 ‘ *Tm ****** 11.80 12.00 12.20 12.40 355 m/z 355.10 33.00% 45

miz-> 0- -24 50 96 100 133 165,193 —T 150 200 250 293 323 E’IAITEI 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 355 11.80 12.00 12'20 12.40 267 m/z 356.10 13.24% 5000

45 207 323, 0- L % ' ■ ■ i ■ • ■“r1 1 1 "i" Tl/z-> 50 100 150 200 250 300 350 Abundance #227689: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... M 73 T T •‘‘I T 11.80 12.00 12.20 12.40 m/z 268.00 10.65%

267 5000

45 135 103 0- 18 A , .7 1 233 ' —r ,92 1 150 1 1 1 1 1 1 ' 1 1 ' T \ T ’ •i m/z—> 50 ' 200 ' 250 100 300 350 11.80 12.00 12.20 12.40

214LB.D 5080302.M Mon Mar 25 08:59:16 2002 Page 4

NYC-WTC_000011355

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NYC-WTC_000011355Source: NYC Law Department, mirrored locally

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