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GCMS analysis results for sample AE03801, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.

NYC-WTC_000037906–000037926

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 12.05 1.76 ug/L 825886 Naphthalene-d8 13.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 62 3 Benzoic acid, 2,6-bis[(trimethyl... 370 C16H30O4Si3 003782-85-2 47 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 43 Abundance Scan 989 (12.046 min): 3801 .D (-) m/z 73.10 100.00% 73

5000 267 355 . _____ t‘ •t ■ I ■ ' • 1 l ‘ ‘

45 11.80 12.00 12.20 12.40 0- - 50 — 108 । i 133 *IIt*162 193 —rh 233—42293 323 +4 m/z 267.00 35.78% m/z-> 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 '' 11.80 12.00 12.20 12.40 m/z 355.10 24.23% 45 207 , 323 , | miz—> 0- ‘I 50 100 150 200 — —250 4— 300 3 +3501 — Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T T 11.80 12.00 12.20 12.40 5000 m/z 356.10 10.00% 267 355 45 01 ,• 1 ,1 1 1■ • 293. ,1 323 i 96 133 165.123223 247, 293 | TT ' IT ■n/z-> 50 100 150 200 250 300 350 Abundance #313257: Benzoic add, 2,6-bis[(trimethylsilyl)oxy]-, trim... 73 355 11*80 12*00 12.20 12.40 m/z74.10 9.40%

5000

147 267 441, . 95 1191 179 207 • 2f7 . 0 TL 4- -4— , 313 i • ‘ ■ 1i —Hr .. \.... m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40 201 n Knnmno M ’Th1 M= 21 11.42.10 anno PaoA 4

NYC-WTC_000037914

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NYC-WTC_000037914Source: NYC Law Department, mirrored locally

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