GCMS analysis report, sample AE02338, March 22, 2002

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Data File : C:\MSDCHEM\1\DATA\030402\2338.D Vial: 10 Acq On : 4 Mar 2002 5:38 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise : Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.08 2.81 ug/L 1237080 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 000541-02-6 90 370 C10H3005Si5 2 Cyclopentasiloxane, decamethyl- 000541-02-6 68 370 C10H3005Si5 3 Phenethylamine, N-methyl-.beta., .. . 399 C18H37NO3Si3 010538-85-9 47 4 N-(Trifluoroacetyl)-0,0',O’'-tri... 481 C19H34F3NO4Si3 000000-00-0 38 Abundance Scan 993 (12.082 min): 2338.D (-) m/z 73.10 100.00% 73

5000 267 355

'11 ‘ 1 ■•i n ।।. 45 11.80 12.00 12.20 12.40 - 108 133154 ,193, 223 1 25 293 323. m/z 267.00 49.22% 0- 1-1 |' 'l Tl-I •|1l‘ l ri 1* T 1-4 t' rr I ’ ' ' * I —r m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 mmmmmor 11.80 12.00 12.20 12.40 m/z 355.10 41.34% 45. 207 , 323 , I । - 0- ■ ' i • ■ m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

■ ■I'''■ l Y'111 ■ ■ । • 11.80 12.00 12.20 12.40 5000 m/z 356.10 14.06% 267 355 45 0- 96 133 । 165,193223 247, 293 323 , i n/z-> 50 100 150 200 250 300 ' 350 Abundance #331718: Phenethylamine, N-methyl-.beta.>3.4-tris(trimethy... 73 ■ I ■'' ■ i ■' 11.80 12.00 12.20 12.40 m/z 268.00 10.73%

5000' 355

44

A . , 1 ?3 116, 147 193 220 267 294 . 384 01 i' * 35 I i#ih i । , • rhrihti m/z—> 50 100 150 200 250 300 ' '350' ’ ' ' 11.80 12.00 12.20 12.40

2338.D 5080302.M Mon Mar 18 08:32:12 2002 Page 5

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