GCMS analysis results for sample AE03733, March 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031202\3733.D Vial: 59 Acq On : 13 Mar 2002 4:24 am Operator: McLean Sample : SAMPLE 3733 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 1.27 ug/L 649021 Naphthalene-d8 13.03

Hit# of 5 Tentative.- ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 3 Phenethylamine, N-methyl-.beta. .... 399 C18H37NO3S13 010538-85-9 47 4 N-(Trifluoroajetetyl)-0,0’,0"-tri. . . 481 C19H34F3NO4Si3 000000-00-0 38 Abundance 7 Scan 990 (12.056 min): 3733 / (-) m/z73.10100.00% 73 '

5000 267 355 _ ___ — L_ _ ___ 11.80 12.00 12.20 12.40 45 108 133154 1?3 223 4 323 m/z 267.00 46.65% - ।T 1 11 0- m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 : * * • ’ I T T 11.80 12.00 12.20 12.40 355 m/z 355.10 40.61% 45 0- T-J— , 96 ,133 165 123.223 247 4 293 323 4 m/z-> 50 ' 100 ' ' 150 ‘ ' 200 ‘ 250 ‘ 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

i • • ■ • i T" T 355 11,80 12.00 12.20 12.40 267 m/z 356.10 14.47% 5000

45 207 323, I 0- — ■ ■ # T — 1II—- miz-> 50 ‘ 100 ‘ 150 200 250 300 350 Abundance #331718: Phenethylamine, N-methyl-.beta.,3.4-tris(trirr>ethy... ‘ 1111/88 It ‘ /1/1/1/1 11119 73 11.80 12.00 12.20 12.40 m/z 268.00 10.75% i 5000 355

44

0 *4 । 93 116.147 193 220 267294 384 1 ■ I 1 1 »• 1 m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

3733.D 5080302.M Fri Mar 15 14:27:12 2002 Page 3

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