GCMS analysis results for sample AE03737, March 29, 2002

NYC 9/11 Public Portal Document

3 Library Search Compound Report

< Data File : C:\MSDCHEM\1\DATA\031202\3737.D Vial: 62 Acq On : 13 Mar 2002 7:57 am Operator: McLean Sample : FB 2/19/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.96 ug/L 489813 Naphthalene-d8 13.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 49 3 Phenethylamine, -methyl-.beta.,... 399 C18H37NO3S13 010538-85-9 43 4 Benzeneethanami e, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 Abundance Scan 990 (12.056 mln): 3737.D (-) m/z 73.10 100.00% 73

5000 267 355

" 11.80 12.00 12.20 12.40 miz-> 0- —+ 50 108 133154 I?3 223 , । -i TY 100 323 . 1* —Ir —r -- 11 * 1 150 200 250 300 350 m/z 267.00 47.63%

Abundance #313068: Cyclopentasil , decamethyl- 73

355 267 5000 i ■ ■ ■ ■ i T T 11.80 12.00 12.20 12.40 m/z 355.10 38.81%

45 323 0- „207 | ।_________________ -**1 1 1 I ' 1 " • i • • • ' i • ■ T—--------- m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T 11.80 12.00 12.20 12.40 5000 m/z 356.10 14.49% 267 355 45 0- 1 ‘ i T PT T 223 247,4 293 323 , 1 96 133 165 193 miz—> 50 100 150 200 250 300 1 350 Abundance #331718: Phenethylamine, N-methyl-beta.,3,4-tris(trimethy... 73 r"I 11.8012.0012.20 12.40 > T

m/z 268.00 10.79%

5000 355

44

। 93 116. 147 193 220 267 294 m/z—> 0 r* 50 1 TTHT’T i . TIT Tr T , r 1’T i . 100 150 200 . 250 300 i 350 384 1 ‘ i ‘1111 ■' • • i ■ • ‘ • i • • 11.80 12.00 12.20 12.40

3737.D 5080302.M Fri Mar 15 14:27:29 2002 Page 3

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