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GCMS analysis results for sample AE02149, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02149 conducted on March 21, 2002, showing surrogate compound data.

NYC-WTC_000039000–000039008

Folder label: “GCMS X 3/8/02 A 3/19/02

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Scanned page image, NYC-WTC_000039007
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NYC 9/11 Public Portal Document

Library Search Compound Report $ 4 Data File : C:\MSDCHEM\l\DATA\031802\2149.D Vial: 27 Acq On : 19 Mar 2002 11:26 pm Operator: McLean Sample : GC/MS SCAN 3/8 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.41 ug/L 172786 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 43 3 Benzeneethanamine, N-[ (pentafluo. . . 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 37 Abundance Scan 989 (12.047 min): 2149.D (-) m/z 73.10 100.00% 73

5000 267 355 11.80 12.00 12.20 12.40 118 154 193 m/z 267.00 38.36% m/z-> O-r — ' 1 i ' ' ' ' i ' -23 ■ । i ■ ■ • ■ i ■ ■ ■ ■ । , ■ • ■ । 50 100 150 200 250 300 350. 400. 450 500 550 ■

Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 5000 267 _ A , 11.80 12.00 12.20 12.40 m/z 355.10 28.41%

207 323. 0( TT TIImBn—m—Ton 1 ' i1 ’ i" 1 ■ 1 i 1 1 1 1 I ' 1 1 ' 1 11 ' 1 1 1 1 m/z—> 50 100.150 200 .250 300 350 400 450 500.. 550 Abundance #31 3065: Cyclopentasiloxane, decamethyl- 73

- 11.80 12.00 12.20 12.40 5000 m/z 74.10 10.38% 267

355

103133163193223 1 r iTTITTT > TIT TT-1rt 0- 28 323 1 ‘‘111111111111111T11111111111T m/z-> 50100150 200 250 300 350 400 450 500550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyi)methylen... 73 11.80 12.00 12.20 12.40 355 m/z 356.10 9.36%

5000

0 —444 , 117147177207 ,251241 — •UUB 386 458 548 —mBTTTTr m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

2149.D 5080302.M Wed Mar 20 02:27:52 2002 Page 3

NYC-WTC_000039007

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NYC-WTC_000039007Source: NYC Law Department, mirrored locally

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