GCMS analysis results for sample AE03736, March 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031202\3736.D Vial: 61 Acq On : 13 Mar 2002 7:08 am Operator: McLean Sample : SAMPLE 3736 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.55 ug/L 256159 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo: ane, decamethyl- 37G C10H3005Si5 000541-02-6 68 2 Cyclopentasilo ane, decamethyl- 370 C10H3005Si5 000541-02-6 47 3 Benzeneacetic <acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 47 4 Benzeneethi amine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 Abundance.... Scan 990 (12.055 min): 3736.D (-) m/z73.10 100.00% 73

5000 267 355

1180 12.00 12.20 12*40 45 154 193 223 , 323 0- -L ■ -I -1 - TIT TIr m/z 267 00 48.07% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 1′2111 T T 11.80 12.00 12.20 12.40 355 m/z 355.10 40.81% 45 01 103 133 165 193 223 1 293 323 . । ITT Pr yn i r t". ′ T • l i » j T TT TT m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 I * ‘1 ‘ 1 T T 355 11.80 12.00 12.20 12.40 267 m/z 356. O’O 12.94% 5000

45 207 . 323 0- • • j' • • ■ । • • ■ • । • ■ ' f T —14 r miz—> Abundance 50 100 150 200 250 300 350 400 450 #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... _ ____ 73 111.80 12.00 12.20 12.40 m/z 268.00 11.11%

5000 355

147 47. 193 237 267295 325 384 429457 0 ■ ' TT 1 105 T T — TdIT T 1r 11 1 ” TTIt ' t ■ T T • • i ■ • • ■ i ‘ • • i ■' ■ ■ i ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

3736.D 5080302.M Fri Mar 15 14:27:23 2002 Page 3

NYC-WTC_000037591