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GCMS analysis report, sample AE02341, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02341 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010639–000010650

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report , Data'File C:\MSDCHEM\l\DATA\030402\2341.D Vial: 13 Acq On 4 Mar 2002 8:05 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

12.07 0.71 ug/L 298289 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30OES15 000541-02-6 90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 58 3 Benzeneethanamine, N- [ (pentafluo. . . 563 C24H34F5 3Si3 055429-13-5 38 4 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 37 Abundance Scan 992 (12.074 min): 2341 .D (-) m/z 73.10 100.00% 73

5000 267 355 " l” "I PPTPT 11.80 12.00 12.2012.40 0-H 154, 193 237 TH**pmmmmmmp Lot, 323 m/z 267.00 33.57% ■ ■ i ‘ ■ i ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ... / . t.... t.... 1180 12.00 12.2012.40 m/z355.10 22.00%

207 . 323 0-H —mmmppmr osj* i " > 11 j ri i 111111 | > ।.. 111 mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 / 11.80 12.00 12.20 12.40 5000 m/z 356.10 9.06% 267 355

281 < ! 103133163193223 1 0- TTftr . । 323 1 i , . . , . ( . . 1 1 j r i 11 । 1 i > > । > 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyf)methylen... T T TPTTPT 355 11.80 12.00 12.20 12.40 m/z74.10 8.66%

5000

, L 117147177207 11714(177207 251281 386 458 548 m/z—> 0-44ATmmmmmpmmpmps 1180 12.00 12.20 1240 50 100 150 200 250 300 350 400 450 500 550

2341.D 5080302.M Mon Mar 18 08:33:03 2002 Page 3

NYC-WTC_000010646

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NYC-WTC_000010646Source: NYC Law Department, mirrored locally

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