GCMS surrogate recovery data, sample AE04384, April 2, 2002

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Data File : C:\MSDCHEM\1\DATA\032602\4384FB.D Vial: 37 Acq On : 27 Mar 2002 10:59 am Operator: McLean Sample : SAMPLE 4384 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.45 ug/L 233352 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 47 4 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 47 Abundance Scan 1527 (12.051 min): 4384FB.D (-) m/z 73.10 100.00% 73

5000 267 355

11*80 12.00 12.20 12.40 n/z-> 0- 44+ , 109 154 191 237 mAmmv* 50 100 150 200 323 ■ ’ i ■ • ■ ■ i ■ • ‘ ■ i ■ ■ •' I'1111 11 m/z 267.00 37.21% 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 • ■ i ■ ■ • ■ I *— 11.80 12.00 12.20 12.40 m/z 355.10 30.37%

m/z—> 0- ■ ■ 11111150 50 100 11 207 72 200 250 300 350 400 '456' 500 550 ' Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ।**•*। T 11.80 12.00 12.20 12.40 5000 m/z 356.10 10.60% 267 355

281 । 103133163193223 1 O-H —Tf 1'1—323 3,2nmmBBnuor niz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... ......... 73 T l * ’ • ‘ l • • ITT 11.80 12.00 12.20 12.40 355 m/z74.10 9.66%

5000

117147177207 251281 458 548 n/z—> oU dmmmmmmmmmempmmpt 386 -_ L -- 4 J_ a____ I__i_A__

50 100 150 200 250 300 350 400 450 500 550 p***r T T 11.80 12.00 12.20 12.40

1384FB.D 5080302.M Wed Mar 27 11:56:31 2002 Page 3

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