Laboratory report documenting GCMS analysis of sample AE03734 for unknown compounds conducted on March 29, 2002.
NYC-WTC_000037548–000037556Folder label: “GCMS X 2/19/02 A 3/12/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031202\3734B.D Vial: 60 Acq On : 13 Mar 2002 6:19 am Operator: McLean Sample : SAMPLE 3734 2/19/02 Inst : Instrumen Misa Multipir: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
12.06 0.66 ug/L 317917 Naphthalene-d8 13.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 (91 2 Cyclopentasili ane, decamethyl- 370 C10H3005Si5 000541-02-6 68 3 Benzeneethanal line, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 47 4 N-(Trifluoroacetyl)-N,0,0’,0’ -t... 553 C22H42F3NO4Si4 000000-00-0 43 Abundance Scan 990 (12.056 min): 3734B.D (-) m/z 73.10 100.00% 73
5000 267 355
1 11 ‘ * 1 —... . 11.80 12.00 12.20 12.40 154 193223 . 323 m/z 267.00 42.96% ■ntz-> 0- , , 14 . 50 ---1 ■ • i' TIT 131. T 116’1111 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73
355 267 5000 111.80 12.00 12.20 1Z40 m/z 355.10 41. 16%
207 . 323 0- 1)ummmm m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73
11.80 12.00 12.20 12*40 5000 m/z 356.00 13.60% 267 355
0-— 281 , _ , 103133163.23223 i-1 17 323 I mlz-> 50 100 150 266' '256’ 300 '356' 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 355 J ‘ ’r ’ I ’ ‘ ‘ • I 11.80 12.00 12.20 12.40 II"
m/z 268.00 10.80%
5000
oU + 1 1174717207 . ... ...... 386 458 . 548 m/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12*20 12.40
3734B.D 5080302.M Fri Mar 15 14:27:17 2002 Page 3
NYC-WTC_000037555
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NYC-WTC_000037539
Laboratory report documenting GCMS analysis of sample AE03732 for unknown compounds conducted on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037575
Laboratory report documenting GCMS analysis of sample AE03798 for unknown compounds conducted on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037521
Gas chromatography-mass spectrometry analysis of environmental sample AE03730 performed March 29, 2002, reporting unknown organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037530
Laboratory report documenting GCMS analysis of sample AE03618 for unknown compounds conducted on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037557
Laboratory report documenting GCMS analysis of sample AE03733 for unknown compounds conducted on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039000
Laboratory report documenting GCMS analysis of sample AE02149 conducted on March 21, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038991
Gas chromatography-mass spectrometry analysis of sample AE02148 conducted on 3/21/02, detecting unknown compounds and 2,4-DDD surrogate at 123 ug with MDL of 5.0 ug.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039009
Laboratory report documenting GCMS analysis of sample AE02150 conducted on March 21, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012436
Gas chromatography-mass spectrometry results for sample AE04377 analyzed on April 2, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059359
Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012494
Laboratory record from April 2, 2002 documenting the recovery of surrogate standards for sample AE04384.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011635
Gas chromatography-mass spectrometry analysis report for sample AE03475 identifying other unknown compounds, conducted March 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037496
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037497
Log sheet recording sample extraction parameters including drip rates, volumes, and pH measurements for environmental analysis.
Filed in the same folder
NYC-WTC_000037499
Chromatogram data from a gas chromatography mass spectrometer analyzing the DFTPP calibration standard on March 12, 2002.
Filed in the same folder
NYC-WTC_000037501
Gas chromatography mass spectrometry analysis of environmental sample AE03730 performed March 12, 2002, reporting specific organic compounds.
Filed in the same folder
NYC-WTC_000037505
Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
Filed in the same folder