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GCMS analysis results for sample AE02150, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02150 conducted on March 21, 2002, showing surrogate compound data.

NYC-WTC_000039009–000039017

Folder label: “GCMS X 3/8/02 A 3/19/02

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Scanned page image, NYC-WTC_000039016
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031802\2150.D Vial: 28 Acg On : 20 Mar 2002 12 :15 am Operator: McLean Sample : GC/MS SCAN 3/8 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.70 ug/L 331165 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 70 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 47 4 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI... 573 C24H51NO5S15 000000-00-0 43 Abundance Scan 989 (12.046 min): 2150.D (-) m/ z 73.10 100.00% 73

5000 267 355 11.80 12.00 12.20 12.40 154 193223 , 323 m/z 267.00 35.07% 0- TTm m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ‘———————11111—07 11.80 12.00 12.20 12.40 m/z 355.10 26.50%

0- | । 207 323 ' ’ I ‘ rT T | > । < । | > । > i | i i i < | । । ' i | > । I ‘ 1’1111111111111 I ' ‘ m/z-> 50.. 100 150 20 .. 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

.... L....... 11.80 12.00 12.20 12.40 5000 m/z 356.00 9.36% 267

355

28 । 103133163193223 L 323 TumBDDT TTTru 04 ' T 1 i ' T TTnu—n—TTuuTim m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyljmethylen... 73 ..... 4..... 355 11.80 12.00 12.20 12.40 m/z 74.10 8.37%

5000

0 4' 1 | 117147177207 251281u TT— 386 458 TI—uu—O—ir] 548 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

2150.D 5080302.M Wed Mar 20 07:02:38 2002 Page 3

NYC-WTC_000039016

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NYC-WTC_000039016Source: NYC Law Department, mirrored locally

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