GCMS analysis results for sample AE03804, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3804.D Vial: 14 Acq On : 19 Mar 2002 10:18 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C: \DATABASE\WILEY7N. L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.05 1.36 ug/L 563583 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 62 3 2-TRIMETHYLSILYLAMIN0-1-TRIMETHY... 457 C20H43NO3Si4 068595-65-3 38 4 1,2 -BIS (TRIMETHYLSILYOXY) -4-TRIM. . . 356 C16H3203Si3 000000-00-0 38 Abundance Scan 989 (12.047 min): 3804.D (-) m/z 73.10 100.00% 73

5000 267 355 -... ...... ... " 11.80 12.00 12.20 12.40 ‘ 0- -L 45 119 154 * 193223 , 323 m/z 267.00 35.10% ■ i •1 ■’ ■nr 1+ — —1 tT ■ । • ■ • ■ । ■11 • m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ ■ i • •' • i • ■ ■' i • i ■ ■ 11.8012.0012.2012.40 m/z 355.10 23.18% 45 207 . 323 miz-> 0- - • * i • 1 ■ ' 1 1 1 1 f r 1 f ■' T TTTT’-nt’’11r 50 100 150 200 250 300 350 400 450 500 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

T 11111 TTTTTTTr 11.80 12.00 12.20 12.40 5000 m/z 356.10 9.40% 267 355 45 0 1 1 1 1 , 103 133 165123223, |, 294323, _ m/z—> 50 100 150 200 250 300 350 400 450 500 Abundance#357157:2-TRIMETHYLSILYLAMINO-1-TRIMETHYLSILYLOXY-1-(3 ’,4. \ 73 T T ••■i T 11.80 12.00 12.20 12.40 m/z74.10 8.99% 355 5000 102

45 — 486 0 TIt 179207 —251281 । i325 147mir ___ 382410 442 . i p i . . । , । । , । |। । , m/z—> 50 100 150 200 250 300 350 400 450 500 11.80 12.00 12.20 12.40

3804.D 5080302.M Thu Mar 21 11:48:05 2002 Page 4 NYC-WTC_000037956