GCMS reference analysis results for sample AE03265, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. -Data File : C:\MSDCHEM\1\DATA\031902\3265FB.D Vial: 34 Acq On : 21 Mar 2002, 8:13 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.,

5.56 1.58 ug/L 1242850 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 36 2 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 3-Pentanol, 3-methyl- (CAS) $$ 3... 102 C6H14O 000077-74-7 9 Abundance Scan 274 (5.561 min): 3265FB.D (-) m/z 73.10 100.00% 73

5000

111 > < * 111111 * in’pi ‘ 111 45 5.20 5.40 5.60 5.80 . 87 103 m/z 45.10 15.12% 01 .............. ............. li 1 i ■ 1 I ' 1 1 1 i 1 ' 1 1 n/z-> 20 30 40 50 60 70 80 90 100 110 Abundance #9701: Butane, 2-methoxy-2-methyl- 73

5000 I1***7ar atimrig 55 5.20 5.40 5.60 5.80 43 87 m/z 71.10 7.52% 27 hl 33 III 49—$1671 —e 0+ —TTt 101 Tl/Z-> 20 30 40 50 60 70 80 90 100 110 Abundance #2002: 1-Propene-1-thiol 73 ‘ I ' ‘ ' * I ‘ ‘ ■' ! ' 10011 . l . । . 5.20 5.40 5.60 5.80 5000 m/z69.10 5.16%

43

0+ -374 4955461971 !<•!•!• rf< ri i j i rri | i m/z-> 20 30 40 50 60 70 80 90 100 110 Abundance #9665: 3-Pentanol, 3-methyl- ------PPPT 73 5.20 5.40 5.60 5.80 m/z 74.10 4.95%

5000 55 43

m/z—> 0 20 29 I I i 36., । 30 40 50 +67 I ' ■ i1 60 70 80 87 111 1111 > । > 11 • 90 100 110 ‘I T 5.20 5.40 5.60 5.80 k 3265FB.D 5080302.M Mon Mar 25 09:02:37 2002 Page 3

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