GCMS analysis results for sample AE00838, Feb 4 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00838.D Vial: 2 Acq On : 31 Jan 2002 3:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 2 Butane, 2-methoxy-2-methyl-... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.39 ug/L 202088 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 36 2 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 3 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 36 4 3-(CYCLOHEX-3f-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 28 Abundance Scan 223 (5.920 min): 00838. D (-) m/ z 73.10 100.00% 73

5000 43 55 87 103 5.60 5.80 6.00 620 m/z-> 0 TE0—nnunn—nm 10 20 30 .444 40 50 | 49 ' i ' 60 ' ■ 1 70 1 1 ' 80 4 90 11mT 100 110 rn/z 43.10 25.40% Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 T । . . i . । | 5.60 5.80 6.00 6.20 55 87 m/z 45.10 9.84% 97 45 3 ' ■ 1 1 ■ 1 ■ 1 1 27• I 33 | ' ' 1 ' I ' ' 1 ‘nil Trm । 1 1 I 1 1 1 1 I'1 ' 1 1 1 1 1 rr /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73 A A ............ 5.60 5.80 6.00 6.20 5000 m/z 41.10, 9.11% 55 43 27

n/z-> 01 15 i ■ ■ 1 ■ 10 i 20 L ’ ' I 1 30 ■ i ■ 40 । ■ i 50 lej....... • ITTPTPTT 60 70 80 90 100 110 Abundance #17065: 3-Pentanol, 2,4-dimethyl- N ..... ...... ‘ ‘‘‘‘ I ' ' ' ' I 73 5.60 5.80 6.00 6.20 m/ z 71.10 6.29%

5000 55

43 27

n/z-> o i ' ■ ' 1 i 10 20 • ■ i ’ 30 - 40 50 I1"............. ' 60 70 1.1/83 80 ............... 90 100 110 PP .... A............ 5.60 5.80 6.00 6.20

00838.D SCAN508.M Fri Feb 01 09:19:05 2002 Page 4

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