GCMS analysis results for sample AE00830, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 Butane, 2-methoxy-2-methyl -... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.93 0.51 ug/L 239020 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl - $$ E... 102 C6H140 000994-05-8 36 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 Pentanol, 5-amino-_________________ 103 C5H13NO 002508-29-4 9 Abundance Scan 224 (5.931 min): 00830.D (-) m/z 73.10 100.00% 73

5000 43 T"T 87 103 5.60 5.806.00 6.20 I I 55 । m/ z 24.64% 0 1 remprp 1 1p । rel 1′ —T POTUTTTTTT i ■1111' ■ ■' r ■' 11 43.10 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 A 1110] PITPA 5.60 5.80 6.00 6.20 55 87 m/z 45.10 11.26% 27 45 01 - I ’ 1 ' 1 H ′ ‘ I 1 ''I 1 I ' + T TTT i1 ■ ■11 ■'111'1 ■ ■ i1 ■' ■ i ■ ■ ■' i'1'11 ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.60% 43 27 55 87 113 174 o1-PTTT 11111■I■''1T' Nii..... 'IT*Tt’011m01’1umummmITTTNT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 m/z 71.10 7.09%

5000 43 27 n/z-> 0 <i•>■■i■— 455 ... 1 87 +TTT Pr 113 174 i ■ ■1' i'1 ■ ■ i' " 11 " 111 ■1 ■' i1 ■' ■ i ■ ■ •11'1'1 r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00' 6.20T7T

00830.D SCAN508.M Fri Feb 01 09:18:31 2002 Page 7

NYC-WTC_000052057

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NYC-WTC_000052057Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE00840, Feb 4 2002 · Box DEP Box 28

NYC-WTC_000052108

Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

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