GCMS analysis results for sample AE00309, Jan 2002

NYC 9/11 Public Portal Document

Llprary Search compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\309.D Vial: 8 Acq On : 8 Jan 2002 11:19 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 Butane, 2-methoxy-2-methyl-... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.84 ug/L 1547350 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual r \ 1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 136 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33/ 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12S1 000075-76-3 9 Abundance Scan 220 (5.885 min): 309. D (-) m/ z 73.10 100.00% 73

5000

43 5.60 5.80 6.00 6.20 55 01 ....... 1 11 ’ i ’’’A ■ ■' 'T' PT 87 103 11 ■ j ■ ■ > -1 । i ■ ■ ■' i ■ ■111 ■ ■ ‘ ■ i m/z 43.10 24.17% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 0Ml.1.. 5.60 5.80 6.00 6.20 55 87 m/z 45.10 9.55% 45

n/z-> 27 I 01’TTTI’ 20 TTT 7 ‘I""!'1' +1I0110PTTITTTTIPIIIT 30 40 50 (60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5.60 5.80 6.00 6.20 5000 m/z 41.10 9.38% 43 27 55 87 113 174 0- ■ i' ■' ■ r —TD 11 "Il " 11 ■ । • ■ • ■ । ■ • ■ • । 1 1 ■ ■ । ■ ■ ■ ■ । i ■1 ■ ■ i ■' ■ ■ i TTTTT n/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3Jdioxolan-2-ylpropyl ester - A mrr , 73 5.60 5.80 6.00 6.20 m/z 71.10 6.47% 5000 43 27 55 87 113 174 0 ''I'"1'.......... 'I1' ' i ''111'''' i' 1" ।1 ■ । ■ ■ ■ ■ । ■ 1 ■ । ।••■ • । ■ > >•।■ 1 ■ ■ i » ■ ■ ■ । ■ ' I'1111 ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

309.D SCAN508.M Wed Jan 09 15:17:26 2002 Page 8

NYC-WTC_000051099