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GCMS analysis results for sample AE00309, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051088–000051104

Folder label: “GCMS X 1/7/02 A 1/8/02”

←Page 13 of 17→
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NYC 9/11 Public Portal Document

Library searcn Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN08\309.D Vial: 8 Acq On : 8 J an 2 0 02 11:19 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Pentanone, 4-hydroxy-4-me.. Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.05 0.33 ug/L 103965 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-283 1 2 2-hydroxymethyl -2,3,3-trimethyl-... 116 C6H1202 110933-26-1 64 ; 3 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-2 45/ 4 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-2 39 Abundance Scan 234 (6.045 min): 309. D (-) m/z 43.10 100.00% 43 59

5000

101 5.60 5.80 6.00 6.20 6.40 0 —+,—514/ m I " " I" ’' I" " I 86 TH m/z 59.10 67.09% mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16604: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 43

5000 i ' ' 1 1 i 1..... P1Mr rMYere । । 59 5.60 5.80 6.00 6.20 6.40 m/2 58.00 24.29% — , 101 27 49 ,, 83 | 0 ■ > | 1 1 1 1 | > । , > | I > ' ' | H . ■ 111 TIWTTUTT+ I " " i " ' ■ i" " r " ’ i" 1' i " " r '1' i" 1 ‘ 11" n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16765: 2-hydroxymethyl-2,3,3-trimethyl-oxirane $$ Oxirane... 43 59 A., IA 5.60 5.80 6.00 6.20 6.40 5000 m/z 101.00 16.66% 31 73 85 ol .... 'I1" ■ । ■ ■ ■ ■ । ■ I....... 'll r - H i"'" i ""i IT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #16613: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... i 1 1 1 1 i 1 1 1 1 r1 1 '11 ′′′ 1 ■' i 1 1 1 43 5.60 5.80 6.00 6.20 6.40 m/ z 44.00 8.34% 59 5000 101

71 83 . ...........|H I ""I"".................... 0 "i " ‘11" " i "1' 111" r । — ' 111" 11 A, m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 5.60 5.80 6.00 6.20 6.40

309.D SCAN508.M Wed Jan 09 15:17:26 2002 Page 9

NYC-WTC_000051100

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