GCMS analysis results for sample AE03477, March 2002

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Library Search Compound Report

- .Data File : C:\MSDCHEM\1\DATA\031202\3477.D Vial: 34 Acq On : 12 Mar 2002 4:08 pm Operator: McLean Sample : SAMPLE 3477 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.56 4.52 ug/L 1518250 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 274 (5.561 min): 3477.D (-) m/z 73.10 100.00% 73

5000

■ i ■ • ■ ■ i1 • • ■ i •''11 • • • ■ i' 45 5.20 5.40 5.60 5.80

miz-> •01 lmptmkm 55 .103 Trm 87 ।. >,, । >,,.,..,, ।..,, । >,.. ।.... । 20 30 40 50 60 70 80 90 100.110120130140150160170180 m/z 45.10 14.62%

Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 TIBBmitrr fTTgT 5.20 5.40 5.60 5.80 43 55 87 m/z71.10 7.14% 29 0 ■ I ■ i A ■ al 11 rr 11 up T ..Pj। > 11 m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ■ i ■'' ■ i' ■ • • i ■ •' • i ■ • • • । ■ 5.20 5.40 5.60 5.80 5000 m/z 55.10 4.89%

43 27 55 , 87 113 131 174 0 mtppp— i r[ i ri'i |i 11 > 11 >i > । i’i 111.,., (,...!,,.. ।.,.. । p-m-r m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #9665:3-Pentanol, 3-methyl- 73 11414,9 ‘1 ( agi 5.20 5.40 5.60 5.80 m/z69.10 4.84%

5000 55 43 87 29

m/z—> 0 qmmmmmmh TDmmTOmWTmTmWWTTVTTTMTTTETT 20 30 40 50 60 70 80 90 100110120130140150160170180 5.20 5.40 5.60 5.80

3477.D 5080302.M Fri Mar 15 11:33:26 2002 Page 3

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