GCMS unknown compound analysis, sample AE05513, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031702\5513Q.D Vial: 14 Acq On : 17 Mar 2002 7:24 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.37 ug/L 383273 1,4-Dichlorobenzene-d4 9.54

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 36 2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 36 3 3-Buten-2-ol 72 C4H8O 000598-32-3 9 4 3-Pentanol, 2,4-dimethyl- (CAS) ... 116 C7H16O 000600-36-2 9 Abundance Scan 274 (5.561 min): 5513Q.D (-) m/z 73710 100.00%' 70

5000

' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' H 45 5.20 5.40 5.60 5.80 55 0 I I I I I I 193 m/z 45.10 13.33% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9663: 3-Pentanol, 3-methyi- 73

5000 5.20 5.40 5.60 5.80 55 m/z 55.10 6.51% 45 87 27 39||1 15 J.I I 67i I 0 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9702: Butane, 2-methoxy-2-methyl- SS Ether, methyl tert-p... 73

T-p-n-r-p-r 5.20 5.40 5.60 5.80 5000 m/z 71.10 6.33%

43 55 87 29 ................. 4.|'..35 , Ipl sA 80 '9'0 160 i -io k 0 ry-rVT-Tq-T-rT--r-p-T-T-ryVT'T^^ 80 Tl/Z-> 10 20 30 . 40 50 60 70 Abundance #1623; 3-Buten-2-ol 43 517 5.20 5.40 5.60 5.80 m/z 74.10 4.77%

5000

29 50 I I..........71 0 'I.............I'l'l'' 37| , I 'n/z-> 10 20 30 40 50 60 70 80 90 100 110 5.20 5.40 5.60 5.80

5513Q.D 5080302.M Mon Mar 25 06:54:18 2002 Page 3

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