GCMS analysis results for sample AE03505, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.. Data File : C:\MSDCHEM\1\DATA\031202\3505.D Vial: 37 Acq On : 12 Mar 2002 6:35 pm Operator: McLean Sample : SAMPLE 3505 2/19/02 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 2.99 ug/L 1030310 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, -methyl- 102 C6H140 000077-74-7 9 2 Butane, 2-m thoxy-2-methyl- $$ E. . . 102 C6H140 000994-05-8 9 3 1-Propene-/-thiol 74 C3H6S 000925-89-3 9 4 3 - Pentanol, 3 -methyl - 102 C6H140 000077-74-7 9 Abundance Scan 274 (5.561 min): 3505.D (-) m/z 73.10 100.00% / 73

5000

»:••••|1...t.... ।.,.. ।. 45 5.20 5.40 5.60 5.80

miz-> 0+ ---674 20 30 40 50 60 70 1.——— 80 87 90 103 100 110 m/z 45.10 13.80%

Abundance #9665:3-Pentanol, 3-methyl- 73

5000 —IWTfr 55 5.20 5.40 5.60 5.80 m/z71.10 6.87% 43 87 29 0 ■... Ill 36, h n. 67 i ■ ■ ■ ■ i 1 TTTTTr TIPut ---ITT m/z-> 20 30 40 50 60 70 80 90 100 110 Abundance #9702: Butane, 2-methoxy-2-methyl- SS Ether, methyl tert-p... 73 • i ■ ■ 1 ■ i • ■ ■ ■ i ■ ‘ i • • • ■ i • 5.20 5.40 5.60 5.80 5000 m/z69.10 4.54%

43 55 87 29

iz-> O+ 1 1 ■ ' 11735 l, 20 30 40 -67 50 60 70 -80--PPPP- 80 90 100 110 Abundance #2002: 1-Propene-1-thiol pip* re 11 > 111111 > 73 5.20 5.40 5.60 5.80 m/z55.10 4.36%

5000 43

m/z—> 0- ......... 20 30 37-140 , he4950। .’55.61 67 , I, ' 'I' . ■ . . j’:1! . > । .... । .... । .... । . ii 60 i 70 80 90 100 110 AAAP 5.20 5.40 5.60 5.80

3505.D 5080302.M Fri Mar 15 11:33:40 2002 Page 3

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