GCMS analysis results for sample AE03380, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\032002\3380.D Vial: 38 Acq On : 21 Mar 2002 2:27 pm Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Pentanol, 2,3-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.31 ug/L 1094670 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2,3-dimethyl- 116 C7H160 000595-41-5 9 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 3 Octanal, 7-methoxy-3,7-dimethyl-... 186 C11H22O2 003613-30-7 9 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 9 Abundance Scan 274 (5.561 min): 3380.D (-) m/z 73.10 100.00% 73

5000

• i • • ■ ■ i11 ■ ■ i ■ • ‘ ■ i • ■1 ' i ‘ 45 5.20 5.40 5.60 5.80 87 103 55 , m/z-> 0- -14 20 40 60 1 80 100 120 ■ i ■ 1 • ■ > '■ ■ ■ ■ i • • ■ • i ■ ' 1 1 i ■ 1 1 ' i

140 160 m/z 45.10 15.36%

Abundance #17059: 3-Pentanol, 2,3-dimethyl- 73

43 87 5000 27 55 5.20 5.40 5.60 5.80 m/z71.10 7.49% 101

miz-> 0- । "T’ T"* । L4 20 40 44——80+ +-.41115, 60 100 120 ■, 140 160 .r Abundance #9665: 3-Pentanol, 3-methyl- 73 . WA . 11. 5.20 5.40 5.60 5.80 5000 m/z69.10 5.29% 55 43 87 29 , lli 0-r * i 1 • ■ I, 1 l 1 -41 1 . TTIT T ti/z-> 20 40 60 80 100 120 140 160 Abundance #95640: Octanal, 7-methoxy-3,7-dimethyl- $$ Methoxycitrone... 73 • i ■ ■ ■ • i • ■ ■ ■ i • ■ ■ • i ■ ■ ■ ■ i ■ 5.20 5.40 5.60 5.80 m/ z 55.10 4.66%

5000

, 29 41 55 m/z—> 0 15,2 20 — 4— 40 460 85 95 111121 137। 153 171 i j . 1 . 7 । . 5** . -W—AA—M4— 80 100 120 140 160 5.20 5.40 5.60 5.80

J380.D 5080302.M Mon Mar 25 09:07:01 2002 Page 3

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