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GCMS analysis results for sample AE03384, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE03384 conducted on March 29, 2002.

NYC-WTC_000011547–000011557

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011554
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

.‘Data File : C:\MSDCHEM\1\DATA\032202\3384.D Vial: 42 Acq On : 22 Mar 2002 5:45 pm Operator: McLean Sample : 2/14/02 REINJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L *********** *.* ******************************************************** Peak Number 1 3-Pentanol, 3-methyl- (CAS)... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 2.14 ug/L 1226270 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- (CAS) $$ 3... 102 C6H140 000077-74-7 38 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 3 Borane, dimethoxy- $$ Dimethoxyb. . . 74 C2H7B02 004542-61-4 9 4 1,3-Dioxolane, 2-methyl- $$ 2-Me... 88 C4H802 000497-26-7 9 Abundance Scan 423 (5.565 min): 3384.D (-) m/z 73.20 100.00% 73

5000 43

11 ''' ri i rl •1 i • 1ijs 11. ।. 5.20 5.40 5.60 5.80 6.00

m/z-> 0- 0 • i • • • ■ i ' ■ ■ • t • 10 20 30 nr 547 40 50 60 70 80 90 100 110 87 103 ' 11 • ■ ■ ■ i • • ■ ‘ ■ m/z 43.20 40.11%

Abundance #9667: 3-Pentanol, 3-methyl- (CAS) $$ 3-Methyl-3-pentanol ... 73 55

5000 TTfTprr TOTTTTTTTTT 43 5.20 5.40 5.60 5.80 6.00 m/z 45.20 14.69% 87 0- ■ ■ i • • ■ • i • ■ ■ • i ■ • • ‘i11 4 80 I ' I 1 ,, | 1 1 i 1 | i i i » | r

n/z-> Abundance 0 10 20 30 40 * 50 60 70 #9663: 3-Pentanol, 3-methyl- 90 100 110 73 TITTPIITP 11. 5.20 5.40 5.60 5.80 6.00 5000 m/z 41.20 13.49%

55 45 87 15 4, 391 0- TTIapo—TTpr 97++ 1 • l‘ 1’ 1** n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #1924: Borane, dimethoxy- $$ Dimethoxyborane $$ (CH30)2BH 73 "*14Hrr 5.20 5.40 5.60 5.80 6.00 m/z71.20 7.49% 43 15 5000

29 57

m/z—> 0- 0 1 21 "TH FI ,.1.. 36 , +TP 10 20 30 40 50 60 70 1 ‘ • i • ■ • • i ■ ■ " i • ■ • • i •

80 90 100 110 TTTTTTT 5.20 5.40 5.60 5.80 6.00

3384.D 5080302.M Mon Mar 25 11:19:25 2002 Page 3

NYC-WTC_000011554

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NYC-WTC_000011554Source: NYC Law Department, mirrored locally

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