GCMS blank analysis results, sample AE05238, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\031602\0309LB.D Vial: 14 Acq On 16 Mar 2002 9:31 pm Operator: McLean Sample 3/9 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peale Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.57 1.80 ug/L 510991 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- / 102 C6H14O 000077-74-7 9 2 3-(CYCLOHEX-3'-EN-YL)PI0PANOL $$... 174 C8H14O4 015745-87-6 9 3 Acetic acid, 3-[1,3]diaxolan-2-y... 174 C8H14O4 000000-00-0 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O _______ 000994-05-8 9 /Abundance Scan 275 (5.570 min): 0309LB.D (-) m/z 73.10 100.00% 7)3

5000

45 "T 5.20 5.40 5.60 5.80 6.00 0^ 11 I IOS m/z 45.10 14.18% m '" I ‘I" " I ‘ I '''' I"'' Tl/2-> __ J20 30 40 50 60 70 80 90 100110120130140 150160170180 Abundance! #9665; 3-Pentanol, 3-methyl- 73

5000 55 5.20 5.40 5.60 5.80 6.00 m/z 71.10 6.89% 87 29 Hi 0 ' I" "I' I J 7iT-rTp-rTT|TTTTyrTTTpTT-rjT^^ -n/2-> 20 30 40 50 60 70 80 90 100110120130140 150160170180 4bundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL SS 2-Cyclohexene-1 -p...’ 73

5.20 5.40 5.60 5.80 6.00 5000 m/z 55.10 5.06%

43 27 55 87 113 131 174 0^ m/2-> :20 30 40,50 60 70 80 90 100110120130140 150160170180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 J 5.20 5.40 5.60 5.80 6.00 m/z 69.10 4.37%

5000

43 27 , 55 ,I 87 113 131 174 m/z-> 0 Wr I" ‘ 'I' I" " I'''' I" " I ’"' I ■mm- 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.20 5.40 5.60 5.80 6.00

0309LB.D 5080302.M Wed Mar 20 08:51:58 2002 Page 3

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