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GCMS analysis results for sample AE03474, March 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for sample AE03474 identifying other unknown compounds, conducted March 28, 2002.

NYC-WTC_000011627–000011634

Folder label: “GCMS X 2/19/02 A 3/12/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031202\3474B.D Vial: 31 Acq On : 12 Mar 2002 1:26 pm Operator: McLean Sample : SAMPLE 3474 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 2.81 ug/L 869570 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 Octanal,/7-methoxy-3, 7-dimethyl-... 186 C11H22O2 003613-30-7 9 33-(CYC -31-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 9 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 274 (5.561 mln): 3474B.D (-) m/z 73.10 100.00% 73

5000

45 5.20 5.40 5.60 5.80 ' 1 551 1 * • >1 * 1***1**’ t 0- .... 87 103 < | t i 8*1******E***|* m/z45.10 14.96% Tt/Z-> 20 40 60 80 100 120 140 160 180 Abundance #9665: 3-Pentanol, 3-methyl- 73

5000 ■ i1'1 ‘ 111 frai 55 5.20 5.40 5.60 5.80 m/z71.10 7.20% 43 87 29 0- ——— ao' 100 120 140 160 180 miz-> 20 40 60 Abundance #95640: Octanal, 7-methoxy-3,7-dimethyl- $$ Methoxycitrone... 73

TT T TT 5.20 5.40 5.60 5.80 5000 m/z69.10 5.15%

20 41 55 15 । . । , —lu. .85 95 171 111121 137 153 -rVr-j-r ■ I ■ • ' ' I ‘ ' TdmaBuaTm Lt .«. 0 1 • 1 1 miz—> 20 40 60 80 100 120 140 160 180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ’T T T T V 5.20 5.40 5.60 5.80 m/z55.10 4.74%

5000

43

0 ,55 27 87 -I4 .1 113 131 174 । premA । > I [ । MAAimrip m/z—> • 20 40 60 80 100 120 140 160 180 5.20 5.40 5.60 5.80

3474B.D 5080302.M Fri Mar 15 11:33:11 2002 Page 3

NYC-WTC_000011633

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NYC-WTC_000011633Source: NYC Law Department, mirrored locally

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