GCMS analysis results for sample AE03282, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

•Data File : C:\MSDCHEM\1\DATA\031902\3282.D Vial: 36 Acq On : 21 Mar 2002 11:07 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.37 ug/L 1141760 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36 2 Methane, isothiocyanate- (CAS) $... 73 C2H3NS 000556-61-6 9 3 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 274 (5.561 mln): 3282.D (-) m/z 73.10 100.00% 73

5000

45 ‘I T T 18T 5.20 5.40 5.60 5.80

n/z-> Of ------+-767+ 10 20 30 40 50 60 70 + 87 80 . t 103 I 1 1 • ‘ 1‘***I‘*‘‘1* 90 100 110 m/z 45.10 15.87%

Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 • l • ■ r. ! . . . . | . ,-|-m > | . 5.20 5.40 5.60 5.80 43 55 87 m/z71.10 7.35% 29

m/z-> 0+ 10 --35,7 20 30 40 50 . 67.. , 80 I’t’1 ■ 111" I ■ • i > • ........ . 60 70 80 90 100 110 ■ i1

Abundance #1775: Methane, isothiocyanate- (CAS) $$ Methyl isothiocya... 73 IIuunmmummm 5.20 5.40 5.60 5.80 5000 m/z69.10 4.71%

45 35 27 58 58 miz-> 01 • ■ i ■ ■' • i ■ -H-p 10 20 30 40 50 60 70 80 I )* 90 100 110 Abundance #9663:3-Pentanol, 3-methyl- 73 ‘I T I • ‘ 1 T it 5.20 5.40 5.60 5.80 m/z55.10 4.61%

5000

55 45 87 27 Of 111 341 TIn . „ 67| . — l'l'l | 1 i i > | i i i i | r -AAA-A IIMMAAg /z—> 10 20 30 40 50 60 70 80 90 100 110 5.20 5.40 5.60 5.80

3282.D 5080302.M Mon Mar 25 09:05:08 2002 Page 3

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