GCMS unknown compound analysis, sample AE05307, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\031702\5307.D Vial: 10 Acq On' 17 Mar 2002 4:09 pm Operator: McLean Sample 3/11/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Methane, isothiocyanato- (C... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.57 0.81 ug/L 283289 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, isothiocyanato- (CAS) $... 73 C2H3NS 000556-61-6 9 2 Octanal, 7-methoxy-3,7-dimethyl- ... 186 C11H22O2 003613-30-7 9 3 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 9 flibundance Scan 275 (5.570 min): 5307.D (-) m/z 73.10 100.00% 7|3

5000

45 5.20 5.40 5.60 5.80 6.00 0 I 8,7 103 m/z 45.10 15.43% ■n/z-> 20 40 60 80 100 120 140 160 Abundance #1775: Methane, isothiocyanate- (CAS) S$ Methyl isothiocya... 73

5000 "T 5.20 5.40 5.60 5.80 6.00 45 m/z 71.10 6.55% 35 I I !.,ii II. 58 h H|. , 0 m/z-> 20 40 60 80 100 120 140 160 Abundance #95640: Octanal. 7-methoxy-3.7-dimethyl- SS Mefhoxycitrone... 73 \....

' I ' ' ' ' I ' ' 5.20 5.40 5.60 5.80 6.00 5000 m/z 69.10 5.53%

OQ 41 55 15 29 J, 111 121 137 153 171 0 ' ' ' i ' ' ' ' i ' ' ' ' I ' ' ' ' I Tl/Z-> 20 40 60 80 100 120 140 160 Abundance #9663: 3-Pentanol, 3-methyl- 73 5.20 5.40 5.60 5.80 6.00 m/z 55.10 5.12%

5000

55 45 87 27 ,1 0 1.5 1.1, ,|ll ' ' I ' ' ' ' I'' ' ..... ........... m/z-> 20 40 80 100 120 140 160 5.20 5.40 5.60 5.80 6.00

5307.D 5080302.M Mon Mar 25 06:50:09 2002 Page 3

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