GCMS unknown compound analysis, sample AE05307, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

, Data File : C:\MSDCHEM\l\DATA\031702\5307.D Vial: 10 Acq On : 17 Mar 2002 4:09 pm Operator: McLean Sample : 3/11/02 Inst • Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Pealt Number 2 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.,

12.06 2.53 ug/L 1236410 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 2 N-(Trifluoracetyl)-0,0',O''-tris... 495 C20H36F3N04Si3 054135-51-2 43 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 43 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H40O5Si4 000000-00-0 38 Abundance Scan 990 (12.056 min): 5307.D (-) rn/z 73.10 100.00% 73

5000 267 355

V. ■p-r-n-fT-r- p ' ' ' f 45 11.80 12.00 12.20 12.40 ,293 323'.......................... m/z 267.00 47.65% 0^ - Tl/z-> 50 100 150 200 250 300 .350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11.80 12.00 12.20 12.40 m/z 355.10 41.88% 45 207 323 i 0 ' I'' ’ • 1''' '■ r’’ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #367529: N-(Tfifluoracetyl)-O,O',O“-fris(trimelhyisilyl)e... 73

355 11.80 12.00 12.20 12.40 5000 m/z 356.10 14.19%

45 , IW IjO 1^ 221 251,281 324.......... 480 0 ■ ' I ■ ' T-t-r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 11.80 12.00 12.20 12.40 m/z 268.00 10.97%

5000 355

44

0 ?????? 384 m/z-> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

!307.D 5080302.M Mon Mar 25 06:50:10 2002 Page 4

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