GCMS unknown compound analysis, sample AE05309, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\031702\5309FB.D Vial: 12 Acq On : 17 Mar 2002 5:46 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.83 ug/L 300933 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 47 3 N-(Trifluoracetyl)-0,0',0''-tris... 495 C20H36F3N04Si3 054135-51-2 38 4 Benzeneacetic acid, .alpha.,4-bi... 384 C17H32O4Si3 037148-64-4 38 fiibundance Scan 990 (12.056 min); 5309FB.D (-) m/ z 73.10 100.00%! 7)3

5000 267 355

I ‘ ' I

45 11.80 12.00 12.20 12.40 162 191 223 I 323 m/z 267.00 47.15% •n/z-> 0 A+ 50 100 I-'-' ' t 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 1^ 5000 11.80 12.00 12.20 12.40 m/z 355.10 41.83% 45 207 323 0 I T' Tl/Z-> 50 100 150 200 250 300 350 400 450 Abundance #331718: Phenethylainine, N-methyl-.beta ,3,4-lris(trirnethy... 73

11.80 12.00 12.20 12.40 5000 m/z 356.00 14.10% 355

44

O ' *1 ■' 116,147 193220 267294 384 I ' i • "l ' ■P ni/z-> 50 100 150 200 250 300 350 400 450 Abundance #367529: N-(Trifluoracetyl)-O,O’.O"-tris(trimethylsilyl)e... 7)3 11.80 12.00 12.20 12.40 m/z 357.10 9.60% 355

5000

45 0 j 480 -i-l-r m/z-> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

5309FB.D 5080302.M Mon Mar 25 06:52:21 2002 Page 4

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