GCMS analysis report for sample AE02335, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. • Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.08 2.82 ug/L 1212720 Naphthalene-d8 13.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 47 3 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 38 4 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 37 Abundance Scan 993 (12.083 mln): 2334.D (-) m/z 73.10 100.00% 73

5000 267 355

" I 1 '111' ri l ’ " 11 1 11.80 12.00 12.20 12.40 45 193 ‘ —293 323+ +1 I ■ 223 0- j~ 108 133154 m/z 267.00 48.84% Tl/Z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 PmmmPTTTT 11.80 12.00 12.20 12.40 m/z 355.10 39.97%

0- 45 11 . ,297, 1I1—fm 323 t m/z-> 50 100 150 200 250 300 350 Abundance #331718: Phenethylamine, N-methyf-.beta.,3,4-tris(trimethy... 73

.. I. ■ ■ ■ I / ir....I ■ ■ 11.80 12.00 12.20 12.40 m/z 356.10 13.48% 5000 355

44

93 116 Bh 147 । । < 193 220 267 294 . 384 0- 1 ‘ • " । ", । r i 'i f t*i r ", 1 1 ■ m/z-> 50 100 150 200 250 300 350' Abundance #313065: Cyclopentasiloxane, decamethyl- 73 TImp rp FPpo 11.80 12.00 12.20 12.40 m/z 268.00 10.88%

5000 267 355 45 0- "I 96 T'1"' 133 165,193 223 247,4 293 323 1 m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

2334.D 5080302.M Mon Mar 18 08:30:55 2002 Page 5

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